Synthesis of β-aniline phenylacetone using microwave irradiation

Jun Ping Zhang; Qiu Yu Zhang; Wan Tao Jiang; Xin Yan; Wen Zhao; He Peng Zhang; Lei Han

Synthesis of β-aniline phenylacetone using microwave irradiation

Jun Ping Zhang, Qiu Yu Zhang, Wan Tao Jiang, Xin Yan, Wen Zhao, He Peng Zhang, Lei Han

School of Chemistry and Chemical Engineering

Northwestern Polytechnical University Xian

Research output: Contribution to journal › Article › peer-review

Abstract

With hydrochloric acid as the catalyzer, β-aniline phenylacetone was synthesized with aniline, trioxym-ethylene and acetophenone under microwave irradiation. The influence of hydrochloric acid dosage, the power and time of microwave irradiation on the process was investigated. The product was characterized by its melting point, IR and 1HNMR. The structure of the product is suitable to the product by conventional method.

Original language	English
Pages (from-to)	60-62
Number of pages	3
Journal	Huaxue Gongcheng/Chemical Engineering (China)
Volume	33
Issue number	3
State	Published - Jun 2005

Keywords

Amino ketone
Mannich base
Microwave synthesis

Cite this

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title = "Synthesis of β-aniline phenylacetone using microwave irradiation",

abstract = "With hydrochloric acid as the catalyzer, β-aniline phenylacetone was synthesized with aniline, trioxym-ethylene and acetophenone under microwave irradiation. The influence of hydrochloric acid dosage, the power and time of microwave irradiation on the process was investigated. The product was characterized by its melting point, IR and 1HNMR. The structure of the product is suitable to the product by conventional method.",

keywords = "Amino ketone, Mannich base, Microwave synthesis",

author = "Zhang, {Jun Ping} and Zhang, {Qiu Yu} and Jiang, {Wan Tao} and Xin Yan and Wen Zhao and Zhang, {He Peng} and Lei Han",

year = "2005",

month = jun,

language = "英语",

volume = "33",

pages = "60--62",

journal = "Huaxue Gongcheng/Chemical Engineering (China)",

issn = "1005-9954",

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T1 - Synthesis of β-aniline phenylacetone using microwave irradiation

AU - Zhang, Jun Ping

AU - Zhang, Qiu Yu

AU - Jiang, Wan Tao

AU - Yan, Xin

AU - Zhao, Wen

AU - Zhang, He Peng

AU - Han, Lei

PY - 2005/6

Y1 - 2005/6

N2 - With hydrochloric acid as the catalyzer, β-aniline phenylacetone was synthesized with aniline, trioxym-ethylene and acetophenone under microwave irradiation. The influence of hydrochloric acid dosage, the power and time of microwave irradiation on the process was investigated. The product was characterized by its melting point, IR and 1HNMR. The structure of the product is suitable to the product by conventional method.

AB - With hydrochloric acid as the catalyzer, β-aniline phenylacetone was synthesized with aniline, trioxym-ethylene and acetophenone under microwave irradiation. The influence of hydrochloric acid dosage, the power and time of microwave irradiation on the process was investigated. The product was characterized by its melting point, IR and 1HNMR. The structure of the product is suitable to the product by conventional method.

KW - Amino ketone

KW - Mannich base

KW - Microwave synthesis

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M3 - 文章

AN - SCOPUS:21444455062

SN - 1005-9954

VL - 33

SP - 60

EP - 62

JO - Huaxue Gongcheng/Chemical Engineering (China)

JF - Huaxue Gongcheng/Chemical Engineering (China)

IS - 3

ER -

Synthesis of β-aniline phenylacetone using microwave irradiation

Abstract

Keywords

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