Optimization of Bi-2223 precursor powder prepared by co-precipitation method

Li Jun Cui, Ping Xiang Zhang, Jin Shan Li, Guo Yan, Xiang Hong Liu, Yong Feng

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

1 Scopus citations

Abstract

Bi(Pb)-Sr-Ca-Cu-O(Bi-2223) precursor powder has been prepared by oxalate co-precipitation method with optimum precipitation condition and heat treatment process. The residual ions in the filtrate can be maintained under 0.2 mmol/L by controlling the pH-value and ageing time. The phase compositions include Bi-2212 as a major phase, Bi2201, Ca2PbO4 and AEC after heat treatment at 800 °C/10 h, 820 °C/20 h, 820 °C/25 h in air. The carbon content can be controlled below 100 ppm by annealing at a flowing oxygen atmosphere. Our results shows it can be applied in a large-quantity preparation of Bi-2223 precursor powder.

Original languageEnglish
Title of host publication2015 IEEE International Conference on Applied Superconductivity and Electromagnetic Devices, ASEMD 2015 - Proceedings
PublisherInstitute of Electrical and Electronics Engineers Inc.
Pages617-618
Number of pages2
ISBN (Electronic)9781467381079
DOIs
StatePublished - 15 Apr 2016
EventIEEE International Conference on Applied Superconductivity and Electromagnetic Devices, ASEMD 2015 - Shanghai, China
Duration: 20 Nov 201523 Nov 2015

Publication series

Name2015 IEEE International Conference on Applied Superconductivity and Electromagnetic Devices, ASEMD 2015 - Proceedings

Conference

ConferenceIEEE International Conference on Applied Superconductivity and Electromagnetic Devices, ASEMD 2015
Country/TerritoryChina
CityShanghai
Period20/11/1523/11/15

Keywords

  • Bi2223
  • co-precipitation
  • precursor powder

Fingerprint

Dive into the research topics of 'Optimization of Bi-2223 precursor powder prepared by co-precipitation method'. Together they form a unique fingerprint.

Cite this