Preparation process optimization of heat released 2PZ-PGMA microcapsule-type latent curing agent

Yu Qi; Qiu Yu Zhang; You Qiang Shi; Shan He

doi:10.11868/j.issn.1005-5053.2015.1.009

Preparation process optimization of heat released 2PZ-PGMA microcapsule-type latent curing agent

Yu Qi, Qiu Yu Zhang, You Qiang Shi, Shan He

化学与化工学院

Beijing Institute of Aeronautical Materials

科研成果: 期刊稿件 › 文章 › 同行评审

2 引用（Scopus）

摘要

A novel heat released microcapsule-type latent curing agent was successfully prepared by solvent evaporation technique with 2-phenylimidazole (2PZ) as core material and polyglycidy methacrylate (PGMA) as wall material. Systematic study of the effects of the kind of solvent and oil-water ratio, type and amount of surfactant, the core-shell feed ratio were carried out on the morphology of microcapsules, particle size and distribution, 2PZ content and yield, etc. When the solvent is methylene chloride, oil-water ratio is 4:5, surfactant is 0.4%(mass fraction) SDS and core-shell weight ratio is 1:1, the optimized preparation of the microcapsule curing agent is obtained.

源语言	英语
页（从-至）	51-58
页数	8
期刊	Hangkong Cailiao Xuebao/Journal of Aeronautical Materials
卷	35
期	1
DOI	https://doi.org/10.11868/j.issn.1005-5053.2015.1.009
出版状态	已出版 - 1 2月 2015

访问文件

10.11868/j.issn.1005-5053.2015.1.009

其它文件与链接

链接到 Scopus 的出版物

引用此

@article{cfdf0ce43081404f9319e629c51084ad,

title = "Preparation process optimization of heat released 2PZ-PGMA microcapsule-type latent curing agent",

abstract = "A novel heat released microcapsule-type latent curing agent was successfully prepared by solvent evaporation technique with 2-phenylimidazole (2PZ) as core material and polyglycidy methacrylate (PGMA) as wall material. Systematic study of the effects of the kind of solvent and oil-water ratio, type and amount of surfactant, the core-shell feed ratio were carried out on the morphology of microcapsules, particle size and distribution, 2PZ content and yield, etc. When the solvent is methylene chloride, oil-water ratio is 4:5, surfactant is 0.4%(mass fraction) SDS and core-shell weight ratio is 1:1, the optimized preparation of the microcapsule curing agent is obtained.",

keywords = "Latent curing agent, Microcapsule, Optimization, Solvent evaporation method",

author = "Yu Qi and Zhang, {Qiu Yu} and Shi, {You Qiang} and Shan He",

year = "2015",

month = feb,

day = "1",

doi = "10.11868/j.issn.1005-5053.2015.1.009",

language = "英语",

volume = "35",

pages = "51--58",

journal = "Hangkong Cailiao Xuebao/Journal of Aeronautical Materials",

issn = "1005-5053",

publisher = "Science Press ",

number = "1",

}

TY - JOUR

T1 - Preparation process optimization of heat released 2PZ-PGMA microcapsule-type latent curing agent

AU - Qi, Yu

AU - Zhang, Qiu Yu

AU - Shi, You Qiang

AU - He, Shan

PY - 2015/2/1

Y1 - 2015/2/1

N2 - A novel heat released microcapsule-type latent curing agent was successfully prepared by solvent evaporation technique with 2-phenylimidazole (2PZ) as core material and polyglycidy methacrylate (PGMA) as wall material. Systematic study of the effects of the kind of solvent and oil-water ratio, type and amount of surfactant, the core-shell feed ratio were carried out on the morphology of microcapsules, particle size and distribution, 2PZ content and yield, etc. When the solvent is methylene chloride, oil-water ratio is 4:5, surfactant is 0.4%(mass fraction) SDS and core-shell weight ratio is 1:1, the optimized preparation of the microcapsule curing agent is obtained.

AB - A novel heat released microcapsule-type latent curing agent was successfully prepared by solvent evaporation technique with 2-phenylimidazole (2PZ) as core material and polyglycidy methacrylate (PGMA) as wall material. Systematic study of the effects of the kind of solvent and oil-water ratio, type and amount of surfactant, the core-shell feed ratio were carried out on the morphology of microcapsules, particle size and distribution, 2PZ content and yield, etc. When the solvent is methylene chloride, oil-water ratio is 4:5, surfactant is 0.4%(mass fraction) SDS and core-shell weight ratio is 1:1, the optimized preparation of the microcapsule curing agent is obtained.

KW - Latent curing agent

KW - Microcapsule

KW - Optimization

KW - Solvent evaporation method

UR - http://www.scopus.com/inward/record.url?scp=84923832091&partnerID=8YFLogxK

U2 - 10.11868/j.issn.1005-5053.2015.1.009

DO - 10.11868/j.issn.1005-5053.2015.1.009

M3 - 文章

AN - SCOPUS:84923832091

SN - 1005-5053

VL - 35

SP - 51

EP - 58

JO - Hangkong Cailiao Xuebao/Journal of Aeronautical Materials

JF - Hangkong Cailiao Xuebao/Journal of Aeronautical Materials

IS - 1

ER -

Preparation process optimization of heat released 2PZ-PGMA microcapsule-type latent curing agent

摘要

访问文件

其它文件与链接

指纹

引用此