TY - JOUR
T1 - Crystal structure of 3,4-bis(nitrofurazano) furoxan
AU - Wang, Jun
AU - Dong, Hai Shan
AU - Huang, Yi Gang
AU - Li, Jin Shan
AU - Zhou, Xiao Qing
PY - 2006/10
Y1 - 2006/10
N2 - The single crystal of 3,4-bis(nitrofurazano) furoxan (BNFF) was obtained using acetone as solvent. Its molecular structure was characterized by elemental analysis, IR, MS, 13C NMR and single-crystal X-ray diffraction. The results indicate that BNFF crystal belongs to orthorhombic, space group P212121 with a = 0.6794 (3) nm, b = 1.0755 (5) nm, c = 1.5137 (4) nm, V = 1.1060 (7) nm3, Mr = 312.14, Z=4, Dx = 1.874 g·cm-3, Dc = 1.875 g·cm-3, F(000) = 624, μ(MoKα) = 0.176 mm-1, R1 = 0.0757, wR2 = 0.1206. Three 5-membered furazan rings of BNFF molecule are planar and the dihedral angles between them are 62.16 (0.29)° and 25.67 (0.36)°.
AB - The single crystal of 3,4-bis(nitrofurazano) furoxan (BNFF) was obtained using acetone as solvent. Its molecular structure was characterized by elemental analysis, IR, MS, 13C NMR and single-crystal X-ray diffraction. The results indicate that BNFF crystal belongs to orthorhombic, space group P212121 with a = 0.6794 (3) nm, b = 1.0755 (5) nm, c = 1.5137 (4) nm, V = 1.1060 (7) nm3, Mr = 312.14, Z=4, Dx = 1.874 g·cm-3, Dc = 1.875 g·cm-3, F(000) = 624, μ(MoKα) = 0.176 mm-1, R1 = 0.0757, wR2 = 0.1206. Three 5-membered furazan rings of BNFF molecule are planar and the dihedral angles between them are 62.16 (0.29)° and 25.67 (0.36)°.
KW - 3,4-bis(nitrofurazano) furoxan (BNFF)
KW - Crystal structure
KW - High energetic compound
KW - Organic chemistry
UR - http://www.scopus.com/inward/record.url?scp=33846131916&partnerID=8YFLogxK
M3 - 文章
AN - SCOPUS:33846131916
SN - 1006-9941
VL - 14
SP - 374
EP - 376
JO - Hanneng Cailiao/Chinese Journal of Energetic Materials
JF - Hanneng Cailiao/Chinese Journal of Energetic Materials
IS - 5
ER -