500 gram-grade synthesis of 3-amino-4-aminoximinofurazan

Jun Wang; Hai Shan Dong; Yi Gang Huang; Xiao Qing Zhou; Jin Shan Li

500 gram-grade synthesis of 3-amino-4-aminoximinofurazan

Jun Wang, Hai Shan Dong, Yi Gang Huang, Xiao Qing Zhou, Jin Shan Li

China Academy of Engineering Physics

科研成果: 期刊稿件 › 文章 › 同行评审

11 引用（Scopus）

摘要

A new energetic material compound 3-amino-4-aminoximinofurazan (AAOF) with yield of 72.4% was synthesized by using dicyanopropane as initial material through 4-step continuous reaction by one-pot method. Its molecular structure was characterized by IR, MS, ¹H-NMR, ¹³C-NMR, elemental analysis and UV. A 500 gram-grade synthesis procedure of 3-amino-4-aminoximinofurazan (AAOF) was realized on the basis of the optimized procedure. The synthesis reaction mechanism of AAOF was theoretically deduced and validated.

源语言	英语
页（从-至）	27-28
页数	2
期刊	Hanneng Cailiao/Chinese Journal of Energetic Materials
卷	14
期	1
出版状态	已出版 - 2月 2006
已对外发布	是

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abstract = "A new energetic material compound 3-amino-4-aminoximinofurazan (AAOF) with yield of 72.4% was synthesized by using dicyanopropane as initial material through 4-step continuous reaction by one-pot method. Its molecular structure was characterized by IR, MS, 1H-NMR, 13C-NMR, elemental analysis and UV. A 500 gram-grade synthesis procedure of 3-amino-4-aminoximinofurazan (AAOF) was realized on the basis of the optimized procedure. The synthesis reaction mechanism of AAOF was theoretically deduced and validated.",

keywords = "3-amino-4-aminoximinofurazan (AAOF), Energetic compound, Organic chemistry, Synthesis",

author = "Jun Wang and Dong, {Hai Shan} and Huang, {Yi Gang} and Zhou, {Xiao Qing} and Li, {Jin Shan}",

year = "2006",

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volume = "14",

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T1 - 500 gram-grade synthesis of 3-amino-4-aminoximinofurazan

AU - Wang, Jun

AU - Dong, Hai Shan

AU - Huang, Yi Gang

AU - Zhou, Xiao Qing

AU - Li, Jin Shan

PY - 2006/2

Y1 - 2006/2

N2 - A new energetic material compound 3-amino-4-aminoximinofurazan (AAOF) with yield of 72.4% was synthesized by using dicyanopropane as initial material through 4-step continuous reaction by one-pot method. Its molecular structure was characterized by IR, MS, 1H-NMR, 13C-NMR, elemental analysis and UV. A 500 gram-grade synthesis procedure of 3-amino-4-aminoximinofurazan (AAOF) was realized on the basis of the optimized procedure. The synthesis reaction mechanism of AAOF was theoretically deduced and validated.

AB - A new energetic material compound 3-amino-4-aminoximinofurazan (AAOF) with yield of 72.4% was synthesized by using dicyanopropane as initial material through 4-step continuous reaction by one-pot method. Its molecular structure was characterized by IR, MS, 1H-NMR, 13C-NMR, elemental analysis and UV. A 500 gram-grade synthesis procedure of 3-amino-4-aminoximinofurazan (AAOF) was realized on the basis of the optimized procedure. The synthesis reaction mechanism of AAOF was theoretically deduced and validated.

KW - 3-amino-4-aminoximinofurazan (AAOF)

KW - Energetic compound

KW - Organic chemistry

KW - Synthesis

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M3 - 文章

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SN - 1006-9941

VL - 14

SP - 27

EP - 28

JO - Hanneng Cailiao/Chinese Journal of Energetic Materials

JF - Hanneng Cailiao/Chinese Journal of Energetic Materials

IS - 1

ER -

500 gram-grade synthesis of 3-amino-4-aminoximinofurazan

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