Synthesis, characterization and structure of some arylantimony ferrocenylacrylates

Jin Shan Li; Run Chang Liu; Xin Bao Chi; Guo Cang Wang; Qun Shen Guo

doi:10.1016/j.ica.2003.12.012

Synthesis, characterization and structure of some arylantimony ferrocenylacrylates

Jin Shan Li, Run Chang Liu, Xin Bao Chi, Guo Cang Wang, Qun Shen Guo

Nankai University

Research output: Contribution to journal › Article › peer-review

18 Scopus citations

Abstract

A series of arylantimony ferrocenylacrylates with the formula (C ₅H₅FeC₅H₄CH=CHCO₂) _nSbAr_(5-n) (n=1, 2; Ar =C₆H₅, 4-CH₃C₆H₄, 3-CH₃C₆H ₄, 2-CH₃C₆H₄, 4-FC₆H ₄) have been synthesized and characterized by elemental analysis, IR, ¹H NMR and mass spectra. The crystal structures of C ₅H₅FeC₅H₄CH=CHCO ₂Sb(C₆H₅)₄ (I₁) and (C₅H₅FeC₅H₄CH=CHCO₂) ₂Sb(C₆H₅)₃ (II₁) have been determined by X-ray diffraction.

Original language	English
Pages (from-to)	2176-2180
Number of pages	5
Journal	Inorganica Chimica Acta
Volume	357
Issue number	7
DOIs	https://doi.org/10.1016/j.ica.2003.12.012
State	Published - 10 May 2004
Externally published	Yes

Keywords

Arylantimony
Coordination
Crystal structure
Distorted octahedron
Ferrocenylacrylate
Pentagonal bipyramid

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10.1016/j.ica.2003.12.012

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@article{a358715ab64146a19628ceebab6e06f1,

title = "Synthesis, characterization and structure of some arylantimony ferrocenylacrylates",

abstract = "A series of arylantimony ferrocenylacrylates with the formula (C 5H5FeC5H4CH=CHCO2) nSbAr(5-n) (n=1, 2; Ar =C6H5, 4-CH3C6H4, 3-CH3C6H 4, 2-CH3C6H4, 4-FC6H 4) have been synthesized and characterized by elemental analysis, IR, 1H NMR and mass spectra. The crystal structures of C 5H5FeC5H4CH=CHCO 2Sb(C6H5)4 (I1) and (C5H5FeC5H4CH=CHCO2) 2Sb(C6H5)3 (II1) have been determined by X-ray diffraction.",

keywords = "Arylantimony, Coordination, Crystal structure, Distorted octahedron, Ferrocenylacrylate, Pentagonal bipyramid",

author = "Li, {Jin Shan} and Liu, {Run Chang} and Chi, {Xin Bao} and Wang, {Guo Cang} and Guo, {Qun Shen}",

year = "2004",

month = may,

day = "10",

doi = "10.1016/j.ica.2003.12.012",

language = "英语",

volume = "357",

pages = "2176--2180",

journal = "Inorganica Chimica Acta",

issn = "0020-1693",

publisher = "Elsevier B.V.",

number = "7",

}

TY - JOUR

T1 - Synthesis, characterization and structure of some arylantimony ferrocenylacrylates

AU - Li, Jin Shan

AU - Liu, Run Chang

AU - Chi, Xin Bao

AU - Wang, Guo Cang

AU - Guo, Qun Shen

PY - 2004/5/10

Y1 - 2004/5/10

N2 - A series of arylantimony ferrocenylacrylates with the formula (C 5H5FeC5H4CH=CHCO2) nSbAr(5-n) (n=1, 2; Ar =C6H5, 4-CH3C6H4, 3-CH3C6H 4, 2-CH3C6H4, 4-FC6H 4) have been synthesized and characterized by elemental analysis, IR, 1H NMR and mass spectra. The crystal structures of C 5H5FeC5H4CH=CHCO 2Sb(C6H5)4 (I1) and (C5H5FeC5H4CH=CHCO2) 2Sb(C6H5)3 (II1) have been determined by X-ray diffraction.

AB - A series of arylantimony ferrocenylacrylates with the formula (C 5H5FeC5H4CH=CHCO2) nSbAr(5-n) (n=1, 2; Ar =C6H5, 4-CH3C6H4, 3-CH3C6H 4, 2-CH3C6H4, 4-FC6H 4) have been synthesized and characterized by elemental analysis, IR, 1H NMR and mass spectra. The crystal structures of C 5H5FeC5H4CH=CHCO 2Sb(C6H5)4 (I1) and (C5H5FeC5H4CH=CHCO2) 2Sb(C6H5)3 (II1) have been determined by X-ray diffraction.

KW - Arylantimony

KW - Coordination

KW - Crystal structure

KW - Distorted octahedron

KW - Ferrocenylacrylate

KW - Pentagonal bipyramid

UR - http://www.scopus.com/inward/record.url?scp=1842636459&partnerID=8YFLogxK

U2 - 10.1016/j.ica.2003.12.012

DO - 10.1016/j.ica.2003.12.012

M3 - 文章

AN - SCOPUS:1842636459

SN - 0020-1693

VL - 357

SP - 2176

EP - 2180

JO - Inorganica Chimica Acta

JF - Inorganica Chimica Acta

IS - 7

ER -

Synthesis, characterization and structure of some arylantimony ferrocenylacrylates

Abstract

Keywords

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