Synthesis and microwave absorption enhancement of graphene@Fe 3O4@SiO2@NiO nanosheet hierarchical structures

Lei Wang, Ying Huang, Xu Sun, Haijian Huang, Panbo Liu, Meng Zong, Yan Wang

Research output: Contribution to journalArticlepeer-review

417 Scopus citations

Abstract

Hierarchical structures of graphene@Fe3O4@SiO 2@NiO nanosheets were prepared by combining the versatile sol-gel process with a hydrothermal reaction. Graphene@Fe3O4 composites were first synthesized by the reduction reaction between FeCl 3 and diethylene glycol (DEG) in the presence of GO. Then, graphene@Fe3O4 was coated with SiO2 to obtain graphene@Fe3O4@SiO2. Finally, NiO nanosheets were grown perpendicularly on the surface of graphene@Fe3O 4@SiO2 and graphene@Fe3O4@SiO 2@NiO nanosheet hierarchical structures were formed. Moreover, the microwave absorption properties of both graphene@Fe3O4 and graphene@Fe3O4@SiO2@NiO nanosheets were investigated between 2 and 18 GHz microwave frequency bands. The electromagnetic data demonstrate that graphene@Fe3O4@SiO2@NiO nanosheet hierarchical structures exhibit significantly enhanced microwave absorption properties compared with graphene@Fe3O4, which probably originate from the unique hierarchical structure with a large surface area and high porosity.

Original languageEnglish
Pages (from-to)3157-3164
Number of pages8
JournalNanoscale
Volume6
Issue number6
DOIs
StatePublished - 21 Mar 2014

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