Synthesis and characterization of mesoporous ZnS

Jia Li; Guang Hui Ning; Xiao Peng Zhao

Synthesis and characterization of mesoporous ZnS

Jia Li, Guang Hui Ning, Xiao Peng Zhao

School of Physical Science and Technology

Northwestern Polytechnical University Xian

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

Mesoporous zinc sulfide was synthesized by a natural templating route in which dodecylamine was chosen as the template-directing agent. Transmission electron microscopy (TEM) and nitrogen adsorption-desorption were used to analyze the morphological characteristics of the obtained products. After removing the templates by solvent extraction method, the mesoporous structure remained stably with a high surface area of 223 m²/g and a narrow pore diameter distribution of 4.9 nm. Furthermore, according to the results being from X-ray diffraction, the obtained mesoporous could be indexed to a cubic ZnS structure. Finally, Fourier transform infrared (FT-IR) and thermogravimetric analysis (TGA) were used to investigate the role of organic template played in connecting the obtained mesoporous structure.

Original language	English
Pages (from-to)	606-609
Number of pages	4
Journal	Gongneng Cailiao/Journal of Functional Materials
Volume	36
Issue number	4
State	Published - Apr 2005

Keywords

Dodecylamine
Mesoporous
Template
Zinc sulfide

Cite this

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title = "Synthesis and characterization of mesoporous ZnS",

abstract = "Mesoporous zinc sulfide was synthesized by a natural templating route in which dodecylamine was chosen as the template-directing agent. Transmission electron microscopy (TEM) and nitrogen adsorption-desorption were used to analyze the morphological characteristics of the obtained products. After removing the templates by solvent extraction method, the mesoporous structure remained stably with a high surface area of 223 m2/g and a narrow pore diameter distribution of 4.9 nm. Furthermore, according to the results being from X-ray diffraction, the obtained mesoporous could be indexed to a cubic ZnS structure. Finally, Fourier transform infrared (FT-IR) and thermogravimetric analysis (TGA) were used to investigate the role of organic template played in connecting the obtained mesoporous structure.",

keywords = "Dodecylamine, Mesoporous, Template, Zinc sulfide",

author = "Jia Li and Ning, {Guang Hui} and Zhao, {Xiao Peng}",

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T1 - Synthesis and characterization of mesoporous ZnS

AU - Li, Jia

AU - Ning, Guang Hui

AU - Zhao, Xiao Peng

PY - 2005/4

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N2 - Mesoporous zinc sulfide was synthesized by a natural templating route in which dodecylamine was chosen as the template-directing agent. Transmission electron microscopy (TEM) and nitrogen adsorption-desorption were used to analyze the morphological characteristics of the obtained products. After removing the templates by solvent extraction method, the mesoporous structure remained stably with a high surface area of 223 m2/g and a narrow pore diameter distribution of 4.9 nm. Furthermore, according to the results being from X-ray diffraction, the obtained mesoporous could be indexed to a cubic ZnS structure. Finally, Fourier transform infrared (FT-IR) and thermogravimetric analysis (TGA) were used to investigate the role of organic template played in connecting the obtained mesoporous structure.

AB - Mesoporous zinc sulfide was synthesized by a natural templating route in which dodecylamine was chosen as the template-directing agent. Transmission electron microscopy (TEM) and nitrogen adsorption-desorption were used to analyze the morphological characteristics of the obtained products. After removing the templates by solvent extraction method, the mesoporous structure remained stably with a high surface area of 223 m2/g and a narrow pore diameter distribution of 4.9 nm. Furthermore, according to the results being from X-ray diffraction, the obtained mesoporous could be indexed to a cubic ZnS structure. Finally, Fourier transform infrared (FT-IR) and thermogravimetric analysis (TGA) were used to investigate the role of organic template played in connecting the obtained mesoporous structure.

KW - Dodecylamine

KW - Mesoporous

KW - Template

KW - Zinc sulfide

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M3 - 文章

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SN - 1001-9731

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JO - Gongneng Cailiao/Journal of Functional Materials

JF - Gongneng Cailiao/Journal of Functional Materials

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Synthesis and characterization of mesoporous ZnS

Abstract

Keywords

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