Preparation and properties of ZnSe microspheres

Xiao Qin Wang; Wan Qi Jie; Huan Yong Li; Li Liu; Yi Ping Tan

Preparation and properties of ZnSe microspheres

Xiao Qin Wang, Wan Qi Jie, Huan Yong Li, Li Liu, Yi Ping Tan

School of Materials Sience and Engineering

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

Well dispersed ZnSe microspheres with diameter of 1-4 μm have been prepared in NaOH aqueous solution as reaction medium, N₂H₄·H₂O as reductive assistant at 140 °C for 24 h by hydrothermal synthesis using ZnSO₄·7H₂O and Na₂SeO₃ as source materials. Through SEM, XRD and UV-vis analysis, it was found that the shape of ZnSe crystal was controlled by NaOH and N₂H₄·H₂O and the products of ZnSe microspheres were hollow microspheres which came from the aggregation of ZnSe nanocrystals with mean diameter of 20.7 nm on the surface of N₂ microbubble.

Original language	English
Pages (from-to)	744-748
Number of pages	5
Journal	Rengong Jingti Xuebao/Journal of Synthetic Crystals
Volume	37
Issue number	3
State	Published - Jun 2008

Keywords

Hollow spheres
Hydrothermal synthesis
Microspheres
ZnSe

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title = "Preparation and properties of ZnSe microspheres",

abstract = "Well dispersed ZnSe microspheres with diameter of 1-4 μm have been prepared in NaOH aqueous solution as reaction medium, N2H4·H2O as reductive assistant at 140 °C for 24 h by hydrothermal synthesis using ZnSO4·7H2O and Na2SeO3 as source materials. Through SEM, XRD and UV-vis analysis, it was found that the shape of ZnSe crystal was controlled by NaOH and N2H4·H2O and the products of ZnSe microspheres were hollow microspheres which came from the aggregation of ZnSe nanocrystals with mean diameter of 20.7 nm on the surface of N2 microbubble.",

keywords = "Hollow spheres, Hydrothermal synthesis, Microspheres, ZnSe",

author = "Wang, {Xiao Qin} and Jie, {Wan Qi} and Li, {Huan Yong} and Li Liu and Tan, {Yi Ping}",

year = "2008",

month = jun,

language = "英语",

volume = "37",

pages = "744--748",

journal = "Rengong Jingti Xuebao/Journal of Synthetic Crystals",

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TY - JOUR

T1 - Preparation and properties of ZnSe microspheres

AU - Wang, Xiao Qin

AU - Jie, Wan Qi

AU - Li, Huan Yong

AU - Liu, Li

AU - Tan, Yi Ping

PY - 2008/6

Y1 - 2008/6

N2 - Well dispersed ZnSe microspheres with diameter of 1-4 μm have been prepared in NaOH aqueous solution as reaction medium, N2H4·H2O as reductive assistant at 140 °C for 24 h by hydrothermal synthesis using ZnSO4·7H2O and Na2SeO3 as source materials. Through SEM, XRD and UV-vis analysis, it was found that the shape of ZnSe crystal was controlled by NaOH and N2H4·H2O and the products of ZnSe microspheres were hollow microspheres which came from the aggregation of ZnSe nanocrystals with mean diameter of 20.7 nm on the surface of N2 microbubble.

AB - Well dispersed ZnSe microspheres with diameter of 1-4 μm have been prepared in NaOH aqueous solution as reaction medium, N2H4·H2O as reductive assistant at 140 °C for 24 h by hydrothermal synthesis using ZnSO4·7H2O and Na2SeO3 as source materials. Through SEM, XRD and UV-vis analysis, it was found that the shape of ZnSe crystal was controlled by NaOH and N2H4·H2O and the products of ZnSe microspheres were hollow microspheres which came from the aggregation of ZnSe nanocrystals with mean diameter of 20.7 nm on the surface of N2 microbubble.

KW - Hollow spheres

KW - Hydrothermal synthesis

KW - Microspheres

KW - ZnSe

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M3 - 文章

AN - SCOPUS:48049121720

SN - 1000-985X

VL - 37

SP - 744

EP - 748

JO - Rengong Jingti Xuebao/Journal of Synthetic Crystals

JF - Rengong Jingti Xuebao/Journal of Synthetic Crystals

IS - 3

ER -

Preparation and properties of ZnSe microspheres

Abstract

Keywords

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