Mullitization Behavior of Al2O3-SiO2 coating deposited by CVD

Zhao Feng Chen, Lai Fei Cheng, Li Tong Zhang, Bo Yan, Cong Li

Research output: Contribution to journalArticlepeer-review

Abstract

The aim of the paper is to study the phase composition and the mullitization behavior of the Al2O3-SiO2 coating deposited by CVD at 550°C using AlCl3-SiCl4-H2-CO2 precursor gaseous. The DTA and XRD were used to examine the mullitization behavior of the coating. The as-deposited coating was composed of γ-Al2O3 and amorphous SiO2. The DTA curve has four peaks. The very weak exothermic peak appeared at about 793°C represented the formation of mullite. The first sharp exothermic peak appeared at about 984°C represented the formation of δ-Al2O3. The very weak endothermic peak appeared at about 1240°C represented the formation of α-Al2O3. The second sharp exothermic peak appeared at about 13371 also represented the formation of mullite. The results indicate the CVD process was no-oxidation and the Al2O3-SiO2 coating can become into mullite-alumina coating by heat-treating it at 1350°C for 2 h.

Original languageEnglish
Pages (from-to)34-37
Number of pages4
JournalHangkong Cailiao Xuebao/Journal of Aeronautical Materials
Volume25
Issue number5
StatePublished - Oct 2005

Keywords

  • AlO-SiO
  • Coating
  • CVD
  • Mullitization behavior

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