TY - JOUR
T1 - Microstructure and mechanical properties of C/C composites with a mesophase pitch transition layer
AU - Liu, Hao
AU - Li, Ke Zhi
AU - Li, He Jun
AU - Lu, Jin Hua
AU - Zhai, Yan Qiang
PY - 2008/5
Y1 - 2008/5
N2 - Carbon/carbon (C/C) composites, with a mesophase pitch transition layer between carbon fiber and pyrocarbon, were prepared by two step technique of liquid impregnation-carbonization and chemical vapor infiltration (CVI). The microstructure and mechanical properties of the as-obtained composites were studied by polarized light microscope (PLM), scanning electron microscope (SEM), conventional and high resolution transmission electron microscope (TEM, HRTEM) and mechanical properties tests, respectively. Results show that the mesophase pitch carbon exhibits lamellar structure, while the pyrocarbon exhibits like-crinkle lamellar structure under SEM and the granular structure under TEM. Under HRTEM, the degree of alignment of lattice fringes decreases gradually for mesophase pitch carbon, pyrocarbon and carbon fiber. The non-brittle fracture behavior of the composites is related to multiple crack deflections caused by the multi-interface and micro-cracks within the matrix carbon layer. The flexural strength and the fracture toughness (KIC) of C/C composites are 244 MPa and 9.7 MPa·m1/2, respectively.
AB - Carbon/carbon (C/C) composites, with a mesophase pitch transition layer between carbon fiber and pyrocarbon, were prepared by two step technique of liquid impregnation-carbonization and chemical vapor infiltration (CVI). The microstructure and mechanical properties of the as-obtained composites were studied by polarized light microscope (PLM), scanning electron microscope (SEM), conventional and high resolution transmission electron microscope (TEM, HRTEM) and mechanical properties tests, respectively. Results show that the mesophase pitch carbon exhibits lamellar structure, while the pyrocarbon exhibits like-crinkle lamellar structure under SEM and the granular structure under TEM. Under HRTEM, the degree of alignment of lattice fringes decreases gradually for mesophase pitch carbon, pyrocarbon and carbon fiber. The non-brittle fracture behavior of the composites is related to multiple crack deflections caused by the multi-interface and micro-cracks within the matrix carbon layer. The flexural strength and the fracture toughness (KIC) of C/C composites are 244 MPa and 9.7 MPa·m1/2, respectively.
KW - Carbon/carbon composites
KW - Mechanical properties
KW - Mesophase pitch
KW - Microstructure
KW - Transition layer
UR - http://www.scopus.com/inward/record.url?scp=45449086304&partnerID=8YFLogxK
U2 - 10.3724/SP.J.1077.2008.00486
DO - 10.3724/SP.J.1077.2008.00486
M3 - 文章
AN - SCOPUS:45449086304
SN - 1000-324X
VL - 23
SP - 486
EP - 490
JO - Wuji Cailiao Xuebao/Journal of Inorganic Materials
JF - Wuji Cailiao Xuebao/Journal of Inorganic Materials
IS - 3
ER -