Microscale synthesis of multiblock copolymers using ultrafast RAFT polymerisation

Joji Tanaka; Pratik Gurnani; Alexander B. Cook; Satu Häkkinen; Junliang Zhang; Jie Yang; Andrew Kerr; David M. Haddleton; Sébastien Perrier; Paul Wilson

doi:10.1039/c8py01437j

Microscale synthesis of multiblock copolymers using ultrafast RAFT polymerisation

Joji Tanaka, Pratik Gurnani, Alexander B. Cook, Satu Häkkinen, Junliang Zhang, Jie Yang, Andrew Kerr, David M. Haddleton, Sébastien Perrier, Paul Wilson

Research output: Contribution to journal › Article › peer-review

30 Scopus citations

Abstract

We demonstrate that ultrafast RAFT in the presence of air can be scaled down to 2 μL with good control using microvolume insert vials as the polymerisation vessel. By careful cooling and mixing of the sequential monomers, well-defined pentablock copolymers were generated with a final volume of 10 μL.

Original language	English
Pages (from-to)	1186-1191
Number of pages	6
Journal	Polymer Chemistry
Volume	10
Issue number	10
DOIs	https://doi.org/10.1039/c8py01437j
State	Published - 14 Mar 2019
Externally published	Yes

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title = "Microscale synthesis of multiblock copolymers using ultrafast RAFT polymerisation",

abstract = "We demonstrate that ultrafast RAFT in the presence of air can be scaled down to 2 μL with good control using microvolume insert vials as the polymerisation vessel. By careful cooling and mixing of the sequential monomers, well-defined pentablock copolymers were generated with a final volume of 10 μL.",

author = "Joji Tanaka and Pratik Gurnani and Cook, {Alexander B.} and Satu H{\"a}kkinen and Junliang Zhang and Jie Yang and Andrew Kerr and Haddleton, {David M.} and S{\'e}bastien Perrier and Paul Wilson",

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doi = "10.1039/c8py01437j",

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AU - Tanaka, Joji

AU - Gurnani, Pratik

AU - Cook, Alexander B.

AU - Häkkinen, Satu

AU - Zhang, Junliang

AU - Yang, Jie

AU - Kerr, Andrew

AU - Haddleton, David M.

AU - Perrier, Sébastien

AU - Wilson, Paul

PY - 2019/3/14

Y1 - 2019/3/14

N2 - We demonstrate that ultrafast RAFT in the presence of air can be scaled down to 2 μL with good control using microvolume insert vials as the polymerisation vessel. By careful cooling and mixing of the sequential monomers, well-defined pentablock copolymers were generated with a final volume of 10 μL.

AB - We demonstrate that ultrafast RAFT in the presence of air can be scaled down to 2 μL with good control using microvolume insert vials as the polymerisation vessel. By careful cooling and mixing of the sequential monomers, well-defined pentablock copolymers were generated with a final volume of 10 μL.

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U2 - 10.1039/c8py01437j

DO - 10.1039/c8py01437j

M3 - 文章

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SN - 1759-9954

VL - 10

SP - 1186

EP - 1191

JO - Polymer Chemistry

JF - Polymer Chemistry

IS - 10

ER -

Microscale synthesis of multiblock copolymers using ultrafast RAFT polymerisation

Abstract

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