@inproceedings{8ad10f9a6b7b45d183352be80eff12d7,
title = "Mechanochemical assisted synthesis of titanium silicalite-1",
abstract = "Titanium Silicalite-1 (TS-1) zeolite was successfully synthesized through a mechanochemical assisted processing. In this method, an amorphous silica-titania precursor was firstly prepared through a mechanochemical treatment. TS-1 was then synthesized by the hydrothermal treatment of the silica-titania precursor with tetrapropylammonium bromide (TPABr) as the template. The results of the XRD, UV-vis, and FT-IR spectrum indicated that the titanium atom was incorporated into the amorphous silica-titania precursor during the grinding, and was also retained in the final TS-1 framework after the hydrothermal treatment. SEM image showed that the TS-1 appeared in a shape of elongated prism. The catalytic performance of TS-1 was examined by phenol hydroxylation with hydrogen peroxide as the oxidant. The results indicated that TS-1 synthesized by this method exhibited a good activity.",
keywords = "Mechanochemical treatment, Silica, Titana, Titanium silicalite-1, TPABr",
author = "Jun Zhang and Shengru Qiao",
year = "2013",
doi = "10.4028/www.scientific.net/AMR.652-654.693",
language = "英语",
isbn = "9783037856208",
series = "Advanced Materials Research",
pages = "693--697",
booktitle = "Advances in Materials and Materials Processing",
note = "2012 3rd International Conference on Advances in Materials and Manufacturing Processes, ICAMMP 2012 ; Conference date: 22-12-2012 Through 23-12-2012",
}