TY - JOUR
T1 - Facile synthesis and optical properties of Prussian Blue microcubes and hollow Fe2O3 microboxes
AU - Wu, Qiaofeng
AU - Wu, Guanglei
AU - Wang, Liuding
AU - Hu, Wenlong
AU - Wu, Hongjing
N1 - Publisher Copyright:
© 2014 Elsevier Ltd.
PY - 2015/2
Y1 - 2015/2
N2 - In this paper, we report a novel strategy for the synthesis of Prussian Blue microcubes via hydrothermal conditions by using K3[Fe(CN)6] and glucose for the first time, and then hollow Fe2O3 microboxes have been successfully fabricated by calcination from a Prussian Blue microcube precursors. The phase structures and morphologies were studied using X-ray powder diffraction (XRD), scanning electronic microscopy (SEM), X-ray photoelectron spectroscopy (XPS), and high resolution transmission electron microscopy (HRTEM) with selected area electron diffraction (SAED). The results depict that highly pure and single crystalline monodisperse hollow Fe2O3 microboxes are successfully obtained, which have a diameter ranging from 3 to 5 μm. The optical properties of the Prussian Blue microcubes and hollow Fe2O3 microboxes were observed by photoluminescence spectra.
AB - In this paper, we report a novel strategy for the synthesis of Prussian Blue microcubes via hydrothermal conditions by using K3[Fe(CN)6] and glucose for the first time, and then hollow Fe2O3 microboxes have been successfully fabricated by calcination from a Prussian Blue microcube precursors. The phase structures and morphologies were studied using X-ray powder diffraction (XRD), scanning electronic microscopy (SEM), X-ray photoelectron spectroscopy (XPS), and high resolution transmission electron microscopy (HRTEM) with selected area electron diffraction (SAED). The results depict that highly pure and single crystalline monodisperse hollow Fe2O3 microboxes are successfully obtained, which have a diameter ranging from 3 to 5 μm. The optical properties of the Prussian Blue microcubes and hollow Fe2O3 microboxes were observed by photoluminescence spectra.
KW - Prussian Blue microcubes Hollow FeO microboxes Hydrothermal reaction Oxidative decomposition PL
UR - https://www.scopus.com/pages/publications/84911392858
U2 - 10.1016/j.mssp.2014.10.014
DO - 10.1016/j.mssp.2014.10.014
M3 - 文章
AN - SCOPUS:84911392858
SN - 1369-8001
VL - 30
SP - 476
EP - 481
JO - Materials Science in Semiconductor Processing
JF - Materials Science in Semiconductor Processing
ER -