A dense ZrB2-SiC-Si/SiC-Si coating to protect carbon/carbon composites against oxidation at 1773 K and 1973 K

Lei Zhou; Qiangang Fu; Dou Hu; Jiaping Zhang; Yalong Wei; Jian Zhu; Jingyuan Song; Mingde Tong

doi:10.1016/j.corsci.2021.109331

A dense ZrB₂-SiC-Si/SiC-Si coating to protect carbon/carbon composites against oxidation at 1773 K and 1973 K

Lei Zhou
, Qiangang Fu
, Dou Hu
, Jiaping Zhang
, Yalong Wei
, Jian Zhu
, Jingyuan Song
, Mingde Tong

材料学院

Northwestern Polytechnical University Xian
AECC Shenyang Engine Research Institute

科研成果: 期刊稿件 › 文章 › 同行评审

75 引用（Scopus）

摘要

A dense double layer ZrB₂-SiC-Si/SiC-Si coating with high content of ZrB₂ was designed and fabricated by dipping-carbonization joint gaseous silicon infiltration. This coating can protect C/C substrate from oxidation in air at 1773 K for 500 h with a weight gain of 1.14 %. Such good oxidation protective performance was ascribed to the dense compound silicate oxide layer accompanied by ZrSiO₄/ZrO₂ pinning phases and compressive stress field around ZrB₂ particles during oxidation. Besides, introducing abundant ZrB₂ phase could inhibit the evaporation of silicate glass at 1973 K, which could protect C/C composites for 78 h with a weight loss of 1.16 %.

源语言	英语
文章编号	109331
期刊	Corrosion Science
卷	183
DOI	https://doi.org/10.1016/j.corsci.2021.109331
出版状态	已出版 - 1 5月 2021

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10.1016/j.corsci.2021.109331

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title = "A dense ZrB2-SiC-Si/SiC-Si coating to protect carbon/carbon composites against oxidation at 1773 K and 1973 K",

abstract = "A dense double layer ZrB2-SiC-Si/SiC-Si coating with high content of ZrB2 was designed and fabricated by dipping-carbonization joint gaseous silicon infiltration. This coating can protect C/C substrate from oxidation in air at 1773 K for 500 h with a weight gain of 1.14 \%. Such good oxidation protective performance was ascribed to the dense compound silicate oxide layer accompanied by ZrSiO4/ZrO2 pinning phases and compressive stress field around ZrB2 particles during oxidation. Besides, introducing abundant ZrB2 phase could inhibit the evaporation of silicate glass at 1973 K, which could protect C/C composites for 78 h with a weight loss of 1.16 \%.",

keywords = "C/C composites, Oxidation resistance, Volume expansion, ZrB",

author = "Lei Zhou and Qiangang Fu and Dou Hu and Jiaping Zhang and Yalong Wei and Jian Zhu and Jingyuan Song and Mingde Tong",

note = "Publisher Copyright: {\textcopyright} 2021 Elsevier Ltd",

year = "2021",

month = may,

day = "1",

doi = "10.1016/j.corsci.2021.109331",

language = "英语",

volume = "183",

journal = "Corrosion Science",

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TY - JOUR

T1 - A dense ZrB2-SiC-Si/SiC-Si coating to protect carbon/carbon composites against oxidation at 1773 K and 1973 K

AU - Zhou, Lei

AU - Fu, Qiangang

AU - Hu, Dou

AU - Zhang, Jiaping

AU - Wei, Yalong

AU - Zhu, Jian

AU - Song, Jingyuan

AU - Tong, Mingde

PY - 2021/5/1

Y1 - 2021/5/1

N2 - A dense double layer ZrB2-SiC-Si/SiC-Si coating with high content of ZrB2 was designed and fabricated by dipping-carbonization joint gaseous silicon infiltration. This coating can protect C/C substrate from oxidation in air at 1773 K for 500 h with a weight gain of 1.14 %. Such good oxidation protective performance was ascribed to the dense compound silicate oxide layer accompanied by ZrSiO4/ZrO2 pinning phases and compressive stress field around ZrB2 particles during oxidation. Besides, introducing abundant ZrB2 phase could inhibit the evaporation of silicate glass at 1973 K, which could protect C/C composites for 78 h with a weight loss of 1.16 %.

AB - A dense double layer ZrB2-SiC-Si/SiC-Si coating with high content of ZrB2 was designed and fabricated by dipping-carbonization joint gaseous silicon infiltration. This coating can protect C/C substrate from oxidation in air at 1773 K for 500 h with a weight gain of 1.14 %. Such good oxidation protective performance was ascribed to the dense compound silicate oxide layer accompanied by ZrSiO4/ZrO2 pinning phases and compressive stress field around ZrB2 particles during oxidation. Besides, introducing abundant ZrB2 phase could inhibit the evaporation of silicate glass at 1973 K, which could protect C/C composites for 78 h with a weight loss of 1.16 %.

KW - C/C composites

KW - Oxidation resistance

KW - Volume expansion

KW - ZrB

UR - https://www.scopus.com/pages/publications/85101614336

U2 - 10.1016/j.corsci.2021.109331

DO - 10.1016/j.corsci.2021.109331

M3 - 文章

AN - SCOPUS:85101614336

SN - 0010-938X

VL - 183

JO - Corrosion Science

JF - Corrosion Science

M1 - 109331

ER -

A dense ZrB2-SiC-Si/SiC-Si coating to protect carbon/carbon composites against oxidation at 1773 K and 1973 K

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A dense ZrB₂-SiC-Si/SiC-Si coating to protect carbon/carbon composites against oxidation at 1773 K and 1973 K