Unexpected one-pot method to synthesize spiro[fluorene-9,9′-xanthene] building blocks for blue-light-emitting materials

Ling Hai Xie; Feng Liu; Chao Tang; Xiao Ya Hou; Yu Ran Hua; Qu Li Fan; Wei Huang

doi:10.1021/ol060871z

Unexpected one-pot method to synthesize spiro[fluorene-9,9′-xanthene] building blocks for blue-light-emitting materials

Ling Hai Xie
, Feng Liu
, Chao Tang
, Xiao Ya Hou
, Yu Ran Hua
, Qu Li Fan
, Wei Huang

Fudan University
Nanjing University
National University of Singapore

Research output: Contribution to journal › Article › peer-review

195 Scopus citations

Abstract

An unexpected one-pot synthetic approach toward spiro[fluorene-9,9′- xanthene] (SFX) under excessive MeSO₃H conditions has been developed. The key step involves a thermodynamically controlled cyclization reaction. Blue-light-emitting materials based on SFX building blocks that exhibit high thermal stability have also been synthesized.

Original language	English
Pages (from-to)	2787-2790
Number of pages	4
Journal	Organic Letters
Volume	8
Issue number	13
DOIs	https://doi.org/10.1021/ol060871z
State	Published - 22 Jun 2006
Externally published	Yes

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10.1021/ol060871z

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title = "Unexpected one-pot method to synthesize spiro[fluorene-9,9′-xanthene] building blocks for blue-light-emitting materials",

abstract = "An unexpected one-pot synthetic approach toward spiro[fluorene-9,9′- xanthene] (SFX) under excessive MeSO3H conditions has been developed. The key step involves a thermodynamically controlled cyclization reaction. Blue-light-emitting materials based on SFX building blocks that exhibit high thermal stability have also been synthesized.",

author = "Xie, \{Ling Hai\} and Feng Liu and Chao Tang and Hou, \{Xiao Ya\} and Hua, \{Yu Ran\} and Fan, \{Qu Li\} and Wei Huang",

year = "2006",

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doi = "10.1021/ol060871z",

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journal = "Organic Letters",

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T1 - Unexpected one-pot method to synthesize spiro[fluorene-9,9′-xanthene] building blocks for blue-light-emitting materials

AU - Xie, Ling Hai

AU - Liu, Feng

AU - Tang, Chao

AU - Hou, Xiao Ya

AU - Hua, Yu Ran

AU - Fan, Qu Li

AU - Huang, Wei

PY - 2006/6/22

Y1 - 2006/6/22

N2 - An unexpected one-pot synthetic approach toward spiro[fluorene-9,9′- xanthene] (SFX) under excessive MeSO3H conditions has been developed. The key step involves a thermodynamically controlled cyclization reaction. Blue-light-emitting materials based on SFX building blocks that exhibit high thermal stability have also been synthesized.

AB - An unexpected one-pot synthetic approach toward spiro[fluorene-9,9′- xanthene] (SFX) under excessive MeSO3H conditions has been developed. The key step involves a thermodynamically controlled cyclization reaction. Blue-light-emitting materials based on SFX building blocks that exhibit high thermal stability have also been synthesized.

UR - https://www.scopus.com/pages/publications/33746126194

U2 - 10.1021/ol060871z

DO - 10.1021/ol060871z

M3 - 文章

AN - SCOPUS:33746126194

SN - 1523-7060

VL - 8

SP - 2787

EP - 2790

JO - Organic Letters

JF - Organic Letters

IS - 13

ER -

Unexpected one-pot method to synthesize spiro[fluorene-9,9′-xanthene] building blocks for blue-light-emitting materials

Abstract

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