Solvent-free Fe3O4 nanofluids with N, N, N', N'-tetramethyl-1, 4-butanediamine as canopy

Ping Qu; Yaping Zheng; Ruilu Yang; Yiwei Wu; Peipei Li

Solvent-free Fe₃O₄ nanofluids with N, N, N', N'-tetramethyl-1, 4-butanediamine as canopy

Ping Qu, Yaping Zheng, Ruilu Yang, Yiwei Wu, Peipei Li

School of Chemistry and Chemical Engineering

Northwestern Polytechnical University Xian

Research output: Contribution to journal › Article › peer-review

Abstract

A gemini cationic quaternary ammonium salt surfactant was synthesized through two-step process with fatty alcohol polyoxyethylene ether (AEO-3), thionyl chloride and N, N, N', N'-tetramethyl-1, 4-diaminobutane. Its structure was characterized by FTIR and H1NMR. Fe₃O₄ nanoparticles were modified by surfactant synthesized in the previous stage, and the product was solvent-free Fe₃O₄ nanofluid. The structure of nanofluids was characterized by FTIR. TGA results show that the percent of Fe₃O₄ nanoparticals is 13.1wt%. TEM image shows that the Fe₃O₄ nanoparticles have good dispersion and particle size is 15~20 nm.

Original language	English
Pages (from-to)	81-87
Number of pages	7
Journal	Xibei Gongye Daxue Xuebao/Journal of Northwestern Polytechnical University
Volume	33
Issue number	1
State	Published - 1 Feb 2015

Keywords

Agents
Alcohols
Ammonia
Characterization
Design of experiments
Electric conductivity of fluids
Ethers
Fatty alcohol polyoxyethylene ether
FeO nanoparticles
Fourier transform infrared Spectroscopy
Nanofluids, nanoparticles
Nuclear magnetic resonance spectroscopy
Polyethylene glycols
Quaternary ammonium salt
Salts
Surface active
Surface tension
Thermogravimetric analysis
Transmission electron microscopy

Cite this

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title = "Solvent-free Fe3O4 nanofluids with N, N, N', N'-tetramethyl-1, 4-butanediamine as canopy",

abstract = "A gemini cationic quaternary ammonium salt surfactant was synthesized through two-step process with fatty alcohol polyoxyethylene ether (AEO-3), thionyl chloride and N, N, N', N'-tetramethyl-1, 4-diaminobutane. Its structure was characterized by FTIR and H1NMR. Fe3O4 nanoparticles were modified by surfactant synthesized in the previous stage, and the product was solvent-free Fe3O4 nanofluid. The structure of nanofluids was characterized by FTIR. TGA results show that the percent of Fe3O4 nanoparticals is 13.1wt%. TEM image shows that the Fe3O4 nanoparticles have good dispersion and particle size is 15~20 nm.",

keywords = "Agents, Alcohols, Ammonia, Characterization, Design of experiments, Electric conductivity of fluids, Ethers, Fatty alcohol polyoxyethylene ether, FeO nanoparticles, Fourier transform infrared Spectroscopy, Nanofluids, nanoparticles, Nuclear magnetic resonance spectroscopy, Polyethylene glycols, Quaternary ammonium salt, Salts, Surface active, Surface tension, Thermogravimetric analysis, Transmission electron microscopy",

author = "Ping Qu and Yaping Zheng and Ruilu Yang and Yiwei Wu and Peipei Li",

year = "2015",

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language = "英语",

volume = "33",

pages = "81--87",

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T1 - Solvent-free Fe3O4 nanofluids with N, N, N', N'-tetramethyl-1, 4-butanediamine as canopy

AU - Qu, Ping

AU - Zheng, Yaping

AU - Yang, Ruilu

AU - Wu, Yiwei

AU - Li, Peipei

PY - 2015/2/1

Y1 - 2015/2/1

N2 - A gemini cationic quaternary ammonium salt surfactant was synthesized through two-step process with fatty alcohol polyoxyethylene ether (AEO-3), thionyl chloride and N, N, N', N'-tetramethyl-1, 4-diaminobutane. Its structure was characterized by FTIR and H1NMR. Fe3O4 nanoparticles were modified by surfactant synthesized in the previous stage, and the product was solvent-free Fe3O4 nanofluid. The structure of nanofluids was characterized by FTIR. TGA results show that the percent of Fe3O4 nanoparticals is 13.1wt%. TEM image shows that the Fe3O4 nanoparticles have good dispersion and particle size is 15~20 nm.

AB - A gemini cationic quaternary ammonium salt surfactant was synthesized through two-step process with fatty alcohol polyoxyethylene ether (AEO-3), thionyl chloride and N, N, N', N'-tetramethyl-1, 4-diaminobutane. Its structure was characterized by FTIR and H1NMR. Fe3O4 nanoparticles were modified by surfactant synthesized in the previous stage, and the product was solvent-free Fe3O4 nanofluid. The structure of nanofluids was characterized by FTIR. TGA results show that the percent of Fe3O4 nanoparticals is 13.1wt%. TEM image shows that the Fe3O4 nanoparticles have good dispersion and particle size is 15~20 nm.

KW - Agents

KW - Alcohols

KW - Ammonia

KW - Characterization

KW - Design of experiments

KW - Electric conductivity of fluids

KW - Ethers

KW - Fatty alcohol polyoxyethylene ether

KW - FeO nanoparticles

KW - Fourier transform infrared Spectroscopy

KW - Nanofluids, nanoparticles

KW - Nuclear magnetic resonance spectroscopy

KW - Polyethylene glycols

KW - Quaternary ammonium salt

KW - Salts

KW - Surface active

KW - Surface tension

KW - Thermogravimetric analysis

KW - Transmission electron microscopy

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M3 - 文章

AN - SCOPUS:84923454616

SN - 1000-2758

VL - 33

SP - 81

EP - 87

JO - Xibei Gongye Daxue Xuebao/Journal of Northwestern Polytechnical University

JF - Xibei Gongye Daxue Xuebao/Journal of Northwestern Polytechnical University

IS - 1

ER -

Solvent-free Fe₃O₄ nanofluids with N, N, N', N'-tetramethyl-1, 4-butanediamine as canopy

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Keywords

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