TY - JOUR
T1 - Revealing microstructure evolution in Fe36Ni36Al17Cr10Mo1 eutectic high entropy alloy over a wide range of strain rate at 1180 ℃
AU - Qiu, Yunji
AU - Shi, Xinbo
AU - Liu, Xiaoming
AU - Wang, Han
AU - He, Feng
AU - Li, Junjie
AU - Wang, Zhijun
N1 - Publisher Copyright:
© 2025 Elsevier Ltd
PY - 2025/12
Y1 - 2025/12
N2 - Eutectic high entropy alloys (EHEAs) have received extensive attention owing to their excellent liquidity and comprehensive mechanical properties. Hot processing serves not only as a central process to tailor the microstructure and properties of metallic materials but also as a critical step toward massive fabrication. In this work, the microstructure evolution and dynamic softening mechanisms of the Fe36Ni36Al17Cr10Mo1 EHEA were studied via hot compression tests at 1180 ℃/0.05 s−1 and 1180 ℃/5 s−1. The initial microstructures in both face-centered-cubic (FCC) and B2 phases contained relatively low fraction of high angle grain boundaries (HAGBs) after homogenization. For low and high strain rates, the FCC phase presented discontinuous dynamic recrystallization (DDRX), while the DDRX process exhibited obvious differences in nucleation and growth. The B2 phase showed a stronger dynamic recovery capability. Consequently, the B2 phase underwent softening via continuous dynamic recrystallization (CDRX) at both strain rates. The misorientation distribution of the lamellar and irregular structures in each phase revealed that recrystallization occurred preferentially within the irregular structure in both phases. This work provided important guidance for understanding the microstructure selection in industrial preparation of EHEAs.
AB - Eutectic high entropy alloys (EHEAs) have received extensive attention owing to their excellent liquidity and comprehensive mechanical properties. Hot processing serves not only as a central process to tailor the microstructure and properties of metallic materials but also as a critical step toward massive fabrication. In this work, the microstructure evolution and dynamic softening mechanisms of the Fe36Ni36Al17Cr10Mo1 EHEA were studied via hot compression tests at 1180 ℃/0.05 s−1 and 1180 ℃/5 s−1. The initial microstructures in both face-centered-cubic (FCC) and B2 phases contained relatively low fraction of high angle grain boundaries (HAGBs) after homogenization. For low and high strain rates, the FCC phase presented discontinuous dynamic recrystallization (DDRX), while the DDRX process exhibited obvious differences in nucleation and growth. The B2 phase showed a stronger dynamic recovery capability. Consequently, the B2 phase underwent softening via continuous dynamic recrystallization (CDRX) at both strain rates. The misorientation distribution of the lamellar and irregular structures in each phase revealed that recrystallization occurred preferentially within the irregular structure in both phases. This work provided important guidance for understanding the microstructure selection in industrial preparation of EHEAs.
KW - Dynamic recrystallization
KW - Eutectic high entropy alloys
KW - Hot processing
KW - Microstructure evolution
KW - Stacking fault energy
UR - https://www.scopus.com/pages/publications/105017779482
U2 - 10.1016/j.mtcomm.2025.114000
DO - 10.1016/j.mtcomm.2025.114000
M3 - 文章
AN - SCOPUS:105017779482
SN - 2352-4928
VL - 49
JO - Materials Today Communications
JF - Materials Today Communications
M1 - 114000
ER -