Process Optimization, Microstructure and Mechanical Properties of SiC + TiB₂/AlSi10Mg Composites Fabricated by Laser-Directed Energy Deposition

In this study, TiB₂/AlSi10Mg, 2 wt.% SiC + TiB₂/AlSi10Mg, and 5 wt.% SiC + TiB₂/AlSi10Mg composite powders were prepared via high-energy ball milling. For the first time, TiB₂ and SiC hybrid particle-reinforced aluminum matrix composites (AMCs) were fabricated using the Laser-Directed Energy Deposition (LDED) technique. The effects of processing parameters on the microstructure evolution and mechanical properties were systematically investigated. Using areal energy density as the main variable, the experiments combined microstructural characterization and mechanical testing to elucidate the underlying strengthening and failure mechanisms. The results indicate that both 2 wt.% and 5 wt.% SiC + TiB₂/AlSi10Mg composites exhibit excellent formability, achieving a relative density of 98.9%. However, the addition of 5 wt.% SiC leads to the formation of brittle Al₄C₃ and TiC phases within the matrix. Compared with the LDED-fabricated AlSi10Mg alloy, the tensile strength of the TiB₂/AlSi10Mg composite increased by 21.4%. In contrast, the tensile strengths of the 2 wt.% and 5 wt.% SiC + TiB₂/AlSi10Mg composites decreased by 3.7% and 2.6%, respectively, mainly due to SiC particle agglomeration and the consumption of TiB₂ particles caused by TiC formation. Nevertheless, their elastic moduli were enhanced by 9% and 16.3%, respectively. Fracture analysis revealed that the composites predominantly exhibited ductile fracture characteristics. However, pores larger than 10 μm and SiC/TiB₂ clusters acted as crack initiation sites, inducing stress concentration and promoting the propagation of secondary cracks.