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Hot deformation behavior and microstructure evolution of flaky Ti3AlC2 particles reinforced pure Al composite

  • Zhijun Wang
  • , Qiang Zhang
  • , Linlin Fu
  • , Puzhen Shao
  • , Yongxiao Zhou
  • , Ping Zhu
  • , Hang Su
  • , Gaohui Wu
  • School of Materials Science and Engineering, Harbin Institute of Technology
  • Shaanxi key Laboratory for Performance and Structure Safety of Petroleum Tubular Goods and Equipment Materials

Research output: Contribution to journalArticlepeer-review

26 Scopus citations

Abstract

Optimizing the hot working parameters of metal matrix composites is beneficial for improving the microstructure of the matrix and the distribution of the reinforcements and eliminating materials defects. In this work, the hot deformation behaviors of the 20 vol% flaky Ti3AlC2 particles reinforced pure Al composite at strain rates of 10−3–1 s−1 and temperatures of 350–500 °C were investigated by hot compression tests. Friction correction equations were used to correct the flow stress data. The constitutive equations and processing maps were successfully established. The flow stresses of the Ti3AlC2/Al composite were precisely described through the hyperbolic sine constitutive equation. The true stress exponent was calculated to be 8, similar to the creep process with invariant microstructure. The particle rotation caused by the deformation of the Al matrix led to the alignment of the Ti3AlC2 flakes. The optimum hot working parameters of the composite are in the range of 410–500 °C, 0.18–1 s−1 based on the processing maps. Dynamic recrystallization (DRX) had a higher proportion in the optimum safe region. The high temperature-low strain rate unstable region was associated with superplastic. The instability in the low temperature-low strain rate region stemmed from the interface microcracks generated by the rotation of Ti3AlC2 flakes. The processing map theory can be well correlated with the microstructure evolution of the composite under different deformation parameters.

Original languageEnglish
Article number167118
JournalJournal of Alloys and Compounds
Volume927
DOIs
StatePublished - 15 Dec 2022
Externally publishedYes

Keywords

  • Al matrix composites
  • Hot deformation
  • MAX phases
  • Preferred orientation
  • Processing maps
  • TiAlC

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