Effect of sintering temperature and composition on microstructure and properties of PMS-PZT ceramics

Hong Liang Du; Zhi Bin Pei; Zhi Min Li; Fa Luo; Dong Mei Zhu; Wan Cheng Zhou; Shao Bo Qu

doi:10.1016/S1003-6326(06)60167-2

Effect of sintering temperature and composition on microstructure and properties of PMS-PZT ceramics

Hong Liang Du
, Zhi Bin Pei
, Zhi Min Li
, Fa Luo
, Dong Mei Zhu
, Wan Cheng Zhou
, Shao Bo Qu

School of Materials Sience and Engineering

Research output: Contribution to journal › Article › peer-review

11 Scopus citations

Abstract

The piezoelectric ceramics xPb(Mn_1/3Sb_2/3)O₃-(1-x) Pb(Zr_1/2Ti_1/2)O₃ (abbreviated as PMS-PZT) were synthesized by traditional ceramics process. The effect of sintering temperature and the amount of Pb(Mn_1/3Sb_2/3)O₃ (abbreviated as PMS) on phase structure, microstructure, piezoelectric and dielectric properties of PMS-PZT ceramics was investigated. The results show that the pure perovskite phase is in all ceramics specimens, the phase structure of PMS-PZT ceramics changes from tetragonal phase to single rhombohedral phase with the increasing amount of PMS. The dielectric constant ε_r, Curie temperature T_C, electromechanical coupling factor k_p and piezoelectric constant d₃₃ decrease, whereas the mechanical quality factor Q_m and dielectric loss tanδ increase with the increasing amount of PMS in system. The optimum sintering temperature is 1200-1250°C. It is concluded that the PMS-PZT (x=0.07) ceramics sintered at 1250°C is suitable for high-power piezoelectric transformer. These properties include ε_r=674.8, tanδ=0.00525, k_p=0.658, Q_m=1520, d₃₃=230 pC/N, T_c=275°.

Original language	English
Pages (from-to)	s165-s169
Journal	Transactions of Nonferrous Metals Society of China (English Edition)
Volume	16
Issue number	SUPPL.
DOIs	https://doi.org/10.1016/S1003-6326(06)60167-2
State	Published - Jun 2006

Keywords

Dielectric properties
PMS-PZT piezoelectric ceramics
Perovskite
Piezoelectric properties

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10.1016/S1003-6326(06)60167-2

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@article{fd2a4e6a3dc645a7ac21acfdee77a9c5,

title = "Effect of sintering temperature and composition on microstructure and properties of PMS-PZT ceramics",

abstract = "The piezoelectric ceramics xPb(Mn1/3Sb2/3)O3-(1-x) Pb(Zr1/2Ti1/2)O3 (abbreviated as PMS-PZT) were synthesized by traditional ceramics process. The effect of sintering temperature and the amount of Pb(Mn1/3Sb2/3)O3 (abbreviated as PMS) on phase structure, microstructure, piezoelectric and dielectric properties of PMS-PZT ceramics was investigated. The results show that the pure perovskite phase is in all ceramics specimens, the phase structure of PMS-PZT ceramics changes from tetragonal phase to single rhombohedral phase with the increasing amount of PMS. The dielectric constant εr, Curie temperature TC, electromechanical coupling factor kp and piezoelectric constant d33 decrease, whereas the mechanical quality factor Qm and dielectric loss tanδ increase with the increasing amount of PMS in system. The optimum sintering temperature is 1200-1250°C. It is concluded that the PMS-PZT (x=0.07) ceramics sintered at 1250°C is suitable for high-power piezoelectric transformer. These properties include εr=674.8, tanδ=0.00525, kp=0.658, Qm=1520, d33=230 pC/N, Tc=275°.",

keywords = "Dielectric properties, PMS-PZT piezoelectric ceramics, Perovskite, Piezoelectric properties",

author = "Du, \{Hong Liang\} and Pei, \{Zhi Bin\} and Li, \{Zhi Min\} and Fa Luo and Zhu, \{Dong Mei\} and Zhou, \{Wan Cheng\} and Qu, \{Shao Bo\}",

year = "2006",

month = jun,

doi = "10.1016/S1003-6326(06)60167-2",

language = "英语",

volume = "16",

pages = "s165--s169",

journal = "Transactions of Nonferrous Metals Society of China (English Edition)",

issn = "1003-6326",

publisher = "Nonferrous Metals Society of China",

number = "SUPPL.",

}

TY - JOUR

T1 - Effect of sintering temperature and composition on microstructure and properties of PMS-PZT ceramics

AU - Du, Hong Liang

AU - Pei, Zhi Bin

AU - Li, Zhi Min

AU - Luo, Fa

AU - Zhu, Dong Mei

AU - Zhou, Wan Cheng

AU - Qu, Shao Bo

PY - 2006/6

Y1 - 2006/6

N2 - The piezoelectric ceramics xPb(Mn1/3Sb2/3)O3-(1-x) Pb(Zr1/2Ti1/2)O3 (abbreviated as PMS-PZT) were synthesized by traditional ceramics process. The effect of sintering temperature and the amount of Pb(Mn1/3Sb2/3)O3 (abbreviated as PMS) on phase structure, microstructure, piezoelectric and dielectric properties of PMS-PZT ceramics was investigated. The results show that the pure perovskite phase is in all ceramics specimens, the phase structure of PMS-PZT ceramics changes from tetragonal phase to single rhombohedral phase with the increasing amount of PMS. The dielectric constant εr, Curie temperature TC, electromechanical coupling factor kp and piezoelectric constant d33 decrease, whereas the mechanical quality factor Qm and dielectric loss tanδ increase with the increasing amount of PMS in system. The optimum sintering temperature is 1200-1250°C. It is concluded that the PMS-PZT (x=0.07) ceramics sintered at 1250°C is suitable for high-power piezoelectric transformer. These properties include εr=674.8, tanδ=0.00525, kp=0.658, Qm=1520, d33=230 pC/N, Tc=275°.

AB - The piezoelectric ceramics xPb(Mn1/3Sb2/3)O3-(1-x) Pb(Zr1/2Ti1/2)O3 (abbreviated as PMS-PZT) were synthesized by traditional ceramics process. The effect of sintering temperature and the amount of Pb(Mn1/3Sb2/3)O3 (abbreviated as PMS) on phase structure, microstructure, piezoelectric and dielectric properties of PMS-PZT ceramics was investigated. The results show that the pure perovskite phase is in all ceramics specimens, the phase structure of PMS-PZT ceramics changes from tetragonal phase to single rhombohedral phase with the increasing amount of PMS. The dielectric constant εr, Curie temperature TC, electromechanical coupling factor kp and piezoelectric constant d33 decrease, whereas the mechanical quality factor Qm and dielectric loss tanδ increase with the increasing amount of PMS in system. The optimum sintering temperature is 1200-1250°C. It is concluded that the PMS-PZT (x=0.07) ceramics sintered at 1250°C is suitable for high-power piezoelectric transformer. These properties include εr=674.8, tanδ=0.00525, kp=0.658, Qm=1520, d33=230 pC/N, Tc=275°.

KW - Dielectric properties

KW - PMS-PZT piezoelectric ceramics

KW - Perovskite

KW - Piezoelectric properties

UR - https://www.scopus.com/pages/publications/33746851633

U2 - 10.1016/S1003-6326(06)60167-2

DO - 10.1016/S1003-6326(06)60167-2

M3 - 文章

AN - SCOPUS:33746851633

SN - 1003-6326

VL - 16

SP - s165-s169

JO - Transactions of Nonferrous Metals Society of China (English Edition)

JF - Transactions of Nonferrous Metals Society of China (English Edition)

IS - SUPPL.

ER -

Effect of sintering temperature and composition on microstructure and properties of PMS-PZT ceramics

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Keywords

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