Abstract
Crack-free zirconia ceramics were consolidated via sintering by intense thermal radiation (SITR) approach at 1600–1700°C for 3–5 min. The resulted ceramic bulks can achieve a relative density up to 99.6% with a grain size of 300–1200 nm. Their bending strength, Vickers hardness and indentation toughness values are up to 1244 ± 139 MPa, 13.3 ± 0.3 GPa and 5.5 ± 0.1 MPa m 1/2 , respectively. Quantitative Raman and XRD analysis show the presence of minor m phase on the natural surface (<7%), fracture surface (<10%) and indentation areas (<15%). It reveals that the SITR method is efficient for rapidly manufacturing zirconia ceramics with desired density, fine grained microstructure and good mechanical properties that are strongly demanded in dental applications.
| Original language | English |
|---|---|
| Pages (from-to) | 23-29 |
| Number of pages | 7 |
| Journal | Advances in Applied Ceramics |
| Volume | 118 |
| Issue number | 1-2 |
| DOIs | |
| State | Published - 17 Feb 2019 |
Keywords
- Bioceramics
- Vickers hardness
- mechanical properties
- microstructure
- sintering by intense thermal radiation (SITR)
- spark plasma sintering
- toughness
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