Dense and strong ZrO 2 ceramics fully densified in <15 min

Duan Li, Yongsheng Liu, Yuan Zhong, Leifeng Liu, Erik Adolfsson, Zhijian Shen

Research output: Contribution to journalArticlepeer-review

13 Scopus citations

Abstract

Crack-free zirconia ceramics were consolidated via sintering by intense thermal radiation (SITR) approach at 1600–1700°C for 3–5 min. The resulted ceramic bulks can achieve a relative density up to 99.6% with a grain size of 300–1200 nm. Their bending strength, Vickers hardness and indentation toughness values are up to 1244 ± 139 MPa, 13.3 ± 0.3 GPa and 5.5 ± 0.1 MPa m 1/2 , respectively. Quantitative Raman and XRD analysis show the presence of minor m phase on the natural surface (<7%), fracture surface (<10%) and indentation areas (<15%). It reveals that the SITR method is efficient for rapidly manufacturing zirconia ceramics with desired density, fine grained microstructure and good mechanical properties that are strongly demanded in dental applications.

Original languageEnglish
Pages (from-to)23-29
Number of pages7
JournalAdvances in Applied Ceramics
Volume118
Issue number1-2
DOIs
StatePublished - 17 Feb 2019

Keywords

  • Bioceramics
  • mechanical properties
  • microstructure
  • sintering by intense thermal radiation (SITR)
  • spark plasma sintering
  • toughness
  • Vickers hardness

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