500 gram-grade synthesis of 3-amino-4-aminoximinofurazan

Jun Wang; Hai Shan Dong; Yi Gang Huang; Xiao Qing Zhou; Jin Shan Li

500 gram-grade synthesis of 3-amino-4-aminoximinofurazan

Jun Wang
, Hai Shan Dong
, Yi Gang Huang
, Xiao Qing Zhou
, Jin Shan Li

China Academy of Engineering Physics

Research output: Contribution to journal › Article › peer-review

11 Scopus citations

Abstract

A new energetic material compound 3-amino-4-aminoximinofurazan (AAOF) with yield of 72.4% was synthesized by using dicyanopropane as initial material through 4-step continuous reaction by one-pot method. Its molecular structure was characterized by IR, MS, ¹H-NMR, ¹³C-NMR, elemental analysis and UV. A 500 gram-grade synthesis procedure of 3-amino-4-aminoximinofurazan (AAOF) was realized on the basis of the optimized procedure. The synthesis reaction mechanism of AAOF was theoretically deduced and validated.

Original language	English
Pages (from-to)	27-28
Number of pages	2
Journal	Hanneng Cailiao/Chinese Journal of Energetic Materials
Volume	14
Issue number	1
State	Published - Feb 2006
Externally published	Yes

Keywords

3-amino-4-aminoximinofurazan (AAOF)
Energetic compound
Organic chemistry
Synthesis

Cite this

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title = "500 gram-grade synthesis of 3-amino-4-aminoximinofurazan",

abstract = "A new energetic material compound 3-amino-4-aminoximinofurazan (AAOF) with yield of 72.4\% was synthesized by using dicyanopropane as initial material through 4-step continuous reaction by one-pot method. Its molecular structure was characterized by IR, MS, 1H-NMR, 13C-NMR, elemental analysis and UV. A 500 gram-grade synthesis procedure of 3-amino-4-aminoximinofurazan (AAOF) was realized on the basis of the optimized procedure. The synthesis reaction mechanism of AAOF was theoretically deduced and validated.",

keywords = "3-amino-4-aminoximinofurazan (AAOF), Energetic compound, Organic chemistry, Synthesis",

author = "Jun Wang and Dong, \{Hai Shan\} and Huang, \{Yi Gang\} and Zhou, \{Xiao Qing\} and Li, \{Jin Shan\}",

year = "2006",

month = feb,

language = "英语",

volume = "14",

pages = "27--28",

journal = "Hanneng Cailiao/Chinese Journal of Energetic Materials",

issn = "1006-9941",

publisher = "Institute of Chemical Materials, China Academy of Engineering Physics",

number = "1",

}

TY - JOUR

T1 - 500 gram-grade synthesis of 3-amino-4-aminoximinofurazan

AU - Wang, Jun

AU - Dong, Hai Shan

AU - Huang, Yi Gang

AU - Zhou, Xiao Qing

AU - Li, Jin Shan

PY - 2006/2

Y1 - 2006/2

N2 - A new energetic material compound 3-amino-4-aminoximinofurazan (AAOF) with yield of 72.4% was synthesized by using dicyanopropane as initial material through 4-step continuous reaction by one-pot method. Its molecular structure was characterized by IR, MS, 1H-NMR, 13C-NMR, elemental analysis and UV. A 500 gram-grade synthesis procedure of 3-amino-4-aminoximinofurazan (AAOF) was realized on the basis of the optimized procedure. The synthesis reaction mechanism of AAOF was theoretically deduced and validated.

AB - A new energetic material compound 3-amino-4-aminoximinofurazan (AAOF) with yield of 72.4% was synthesized by using dicyanopropane as initial material through 4-step continuous reaction by one-pot method. Its molecular structure was characterized by IR, MS, 1H-NMR, 13C-NMR, elemental analysis and UV. A 500 gram-grade synthesis procedure of 3-amino-4-aminoximinofurazan (AAOF) was realized on the basis of the optimized procedure. The synthesis reaction mechanism of AAOF was theoretically deduced and validated.

KW - 3-amino-4-aminoximinofurazan (AAOF)

KW - Energetic compound

KW - Organic chemistry

KW - Synthesis

UR - https://www.scopus.com/pages/publications/33645145893

M3 - 文章

AN - SCOPUS:33645145893

SN - 1006-9941

VL - 14

SP - 27

EP - 28

JO - Hanneng Cailiao/Chinese Journal of Energetic Materials

JF - Hanneng Cailiao/Chinese Journal of Energetic Materials

IS - 1

ER -

500 gram-grade synthesis of 3-amino-4-aminoximinofurazan

Abstract

Keywords

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